Minnesota State University Moorhead
Dr. Craig P. Jasperse, Chemistry
Phone: (218) 477-2230            Home: (218) 291-9841 
Office: Hagen407J              email: jasperse@mnstate.edu           fax: (218) 477-2137
Office Hours:   Mon/Wed/Fri: 9-10:30, 1:00-2:00; Tues 10-11:30; Thurs 1:00-2:00

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Chem 355-O1 Lab
Chem 360-Organic 2
Chem 365-O2 Lab

Chem 341-Organic 1
Chem 342-Organic 2
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Full Chem 355 Lab Manual 2018
Chem 355 Syllabus for 2018
       Required Text and Materials for Fall 2018      

Chem 355 Lab Schedule Fall 2018   Full Chem 355 Lab Manual 2018
Ex Dates Experiment Expt. Links Movie Links mp4 Podcasts Links
1 Aug 28-30 Checkin, Melting Points Melting Range Handout Syllabus Movie
Melting Range Movie
Syllabus Podcast
Melting Range Podcast
2 Sept 4-6 Solubility Tests; Crystallization of Phtallic Acid
Recrystallizaton-1 Handout Recrystallizaton-1 Movie Recrystallizaton-1 Podcast
2 Sept 11-13 Molecular Structure Molecular Modelling Handout Molecular Modelling Movie Molecular Modelling Podcast
4 Sept 18-20 Recrystallization of Acetanilide Using Mixed Solvent; Recrystallization of an Unknown Recrystallization-2 Handout Recrystallization-2 Movie Recrystallization-2 Podcast (Podcast is good)
5 Sept 25-27 Simple and Fractional Distillation of a Mixture Distillation Handout Distillation Movie Distillation Podcast
6 Oct. 2-4 Gas Chromatography-Mass Spectrometry (GC-MS) Lab GC-MS Handout GC-MS Movie GC-MS Podcast
7 Oct 9-11 Nucleophilic Substitution of Alkyl Halides
Mechanisms and Arrow Pushing
SN2-SN1 Handout SN2-SN1 Movie SN2-SN1 Podcast
8 Oct 16-18 No Lab This Week No Lab This Week No Lab This Week No Lab This Week
9 Oct 23-25 Chromatography;  TLC, Column, and Flash Chromatography Chromatography Handout Chromatography Movie Chromatography Podcast
10 Oct 30-Nov 1 Separatory Funnel and Rotory Evaporation:
Liquid/liquid Extraction; Extraction of Acids and Bases
Acid-Base Extraction Handout Acid-Base Extraction Movie Acid-Base Extraction Podcast
11 Nov 6-8 13C Nuclear Magnetic Resonance (13C NMR) Spectroscopy C-13 NMR Handout
C-NMR Interpretation (Condensed)
C-13 NMR Movie (prelab, 5-min)

C-13 Full Movie 60-min

C-13 NMR Podcast (prelab, 5-min)

C-13 NMR Podcast (full movie, 60-min)

12 Nov 13-15 1H Nuclear Magnetic Resonance (1H NMR) Spectroscopy
H-NMR Handout
H-NMR Interpretation (Condensed)
H-NMR Movie
H-NMR Podcast
  Nov 20-22 Thanksgiving No Lab even on Tuesday    
13 Nov 27-Nov 29 Diels-Alder Reaction 1.Diels-Alder Reaction
2.Standard Synthesis Report Format
1.Diels-Alder Reaction Movie
2.Standard Synthesis Report Movie

1.Diels-Alder Reaction Podcast
2.Standard Synthesis Report Podcast

14 Nov 28-Nov 30 Nitration of Methyl Benzoate
Cleanup, Checkout
Nitration of Methyl Benzoate Handout Nitration of Methyl Benzoate Movie Nitration of Methyl Benzoate Podcast