Minnesota State University Moorhead
Dr. Craig P. Jasperse, Chemistry
Phone: (218) 477-2230            Home: (218) 291-9841 
Office: Hagen407J              email: jasperse@mnstate.edu           fax: (218) 477-2137
Office Hours:   Mon/Wed/Fri: 9-10:30, 1:00-2:00; Tues 10-11:30; Thurs 1:00-2:00

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Full Chem 355 Lab Manual 2020
Chem 355 Syllabus for 2020
       Required Text and Materials for Fall 2020      

Chem 355 Lab Schedule Fall 2020   Full Chem 355 Lab Manual 2020
Ex Dates Experiment Expt. Links Movie Links  
1 Aug 25,27 Checkin, Melting Points Melting Range Handout Syllabus Movie
Melting Range Movie
2 Sept 1,3 Solubility Tests; Crystallization of Phtallic Acid
Recrystallizaton-1 Handout Recrystallizaton-1 Movie  
2 Sept 8,10 Molecular Structure Molecular Modelling Handout Molecular Modelling Movie  
4 Sept 15,17 Recrystallization of Acetanilide Using Mixed Solvent; Recrystallization of an Unknown Recrystallization-2 Handout Recrystallization-2 Movie  
5 Sept 22,24 Separatory Funnel and Rotory Evaporation:
Liquid/liquid Extraction; Extraction of Acids and Bases
Acid-Base Extraction Handout Acid-Base Extraction Movie  

Sept 29,

Gas Chromatography-Mass Spectrometry (GC-MS) Lab GC-MS Handout GC-MS Movie  
7 Oct 6,8 Nucleophilic Substitution of Alkyl Halides
Mechanisms and Arrow Pushing
SN2-SN1 Handout SN2-SN1 Movie  
8 Oct 13,15 Chromatography;  TLC, Column, and Flash Chromatography Chromatography Handout Chromatography Movie  
9 Oct 20,22 Simple and Fractional Distillation of a Mixture Distillation Handout Distillation Movie  
10 Oct 27,29 C13 Nuclear Magnetic Resonance (C NMR) Spectroscopy C-13 NMR Handout
C-NMR Interpretation (Condensed)
C-13 NMR Movie (prelab, 5-min)

C-13 Full Movie 70-min
11 Nov 3,5 1H Nuclear Magnetic Resonance (1H NMR) Spectroscopy
H-NMR Handout
H-NMR Interpretation (Condensed)
H-NMR Movie
12 Nov 10,12 Diels-Alder Reaction 1.Diels-Alder Reaction
2.Standard Synthesis Report Format
1.Diels-Alder Reaction Movie
2.Standard Synthesis Report Movie
13 Nov 17,19 Nitration of Methyl Benzoate
Cleanup, Checkout
Nitration of Methyl Benzoate Handout Nitration of Methyl Benzoate Movie  
  Nov 24,26 Thanksgiving No Lab even on Tuesday    
  Dec 1,3 No Lab After Thanksgiving No Lab