Minnesota State University Moorhead
Dr. Craig P. Jasperse, Chemistry
Phone: (218) 477-2230            Home: (218) 291-9841 
Office: Hagen407J              email: jasperse@mnstate.edu           fax: (218) 477-2137
Office Hours:   Mon/Wed/Fri: 9-10:30, 1:00-2:00; Tues 10-11:30; Thurs 1:00-2:00

Chem 350-Organic 1
Chem 355-O1 Lab
Chem 360-Organic 2
Chem 365-O2 Lab

Chem 341-Organic 1
Chem 342-Organic 2
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Syllabus Chem 365-2019                   Required Text and Materials        
2019 Complete Lab Manual
Standard Synthesis Lab Report Format
H-NMR Interpretation (Condensed)       H-NMR Interpretation (Longer)       NMR User's Manual
C13-NMR Interpretation (Condensed)        NMR Physics and C13-NMR (Longer)       GC/MS User's Manual

Chem 365 Lab Schedule Spring 2019
Lab times (Langseth 307): Thursday 9am, 1:30pm  

Date Experiment Lab Manual for 2019 (Complete)
PreLab Lectures (Streaming) (Podcast)
Jan 17 Cyalume: Chemiluminescence 1. Cyalume Experiment    
2. Syllabus

3. Standard lab report format
Syllabus and Introduction (8 min)
Cyalume Prelab Lecture (27 min)

Cyalume Prelab Pod
Jan 24 Snowed Out 2019      
Jan 31 Grignard Reactions, Part 1 Grignard Reactions Grignard Prelab Week 1 Grignard1-Pod
Feb 7 Snowed Out 2019      
Feb 14 Grignard Reactions, Part II 1. Grignard Reactions
2. GC-MS User's Sheet
Grignard Prelab Week 2 Grignard2-Pod
Feb 21 Alcohol to Ester; Catalysis; Distillation; NMR 1. Alcohol Esterification Expt
2. H-NMR Interpretation (Summary)
3. H-NMR Interpretation (Detailed)
4. NMR User's Sheet
Alcohol Esterification Prelab Esterification Pod
    NMR Movie: Format for reporting and interpreting H and C NMR Standard Summary Report pod
    NMR Movie: How to find spectra for printing and processing NMR: Finding spectra for printing and processing Pod
Feb 28 Aspirin Synthesis/Alcohol Unknown (NMR) Aspirin, Alcohol NMR Expt 1. Aspirin, Alcohol Prelab
2. NMR: Standard Summary for H or C NMR
3. NMR: Finding spectra for printing and processing
1. Aspirin Pod
2. Standard Summary Report
3. NMR: Finding spectra for printing and processing
Mar 7 Spring Break      
Mar 14 Storm Cancellation      
Mar 21 Aldehydes and Ketones Unknown/Derivative Carbonyl Unknowns Experiment Carbonyl Unknowns Prelab Carbonyl Pod
Mar 28 Dibenzalacetone by Aldol Condensation Aldol Reaction Aldol Prelab Aldol Pod
Apr 4

Multistep Synthesis Module Week One

Research Module 2019

Full Video, 58 min ...
-intro part
-procedure part (26min)
-NMR part (20 min)
Week 1 Pod
Week 2 Pod

Apr 11 Multistep Synthesis Module Week Two

Research Module

Week 2 video
-28 min
2D-NMR helps interpret H-NMR

Multistep 3 Pod
Extra 5-min NMR

Apr 18

 No Lab, Easter      
Apr 25 Amine Unknowns Amines Unknown Experiment Amines Prelab Amines Pod
May 2 Carboxylic Acid Unknown and Titration. Cleanup, Checkout Acid Unknowns Experiment Acid Prelab Acid Pod