Minnesota State University Moorhead
Dr. Craig P. Jasperse, Chemistry
Phone: (218) 477-2230            Home: (218) 291-9841 
Office: Hagen407J              email: jasperse@mnstate.edu           fax: (218) 477-2137
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Full Chem 355 Lab Manual 2022
Chem 355 Syllabus for 2022

       Required Text and Materials for Fall 2022      

Chem 355 Lab Schedule Fall 2021   Full Chem 355 Lab Manual 2022
Ex Dates Experiment Expt. Links Movie Links  
1 Aug 24,25 Checkin, Melting Points Melting Range Handout Syllabus Movie
Melting Range Movie
2 Aug 31, Sept 1 Solubility Tests; Crystallization of Phtallic Acid
Recrystallizaton-1 Handout Recrystallizaton-1 Movie  
2 Sept 7, 8 Molecular Structure Molecular Modelling Handout Molecular Modelling Movie  
4 Sept 14,15 Recrystallization of Acetanilide Using Mixed Solvent; Recrystallization of an Unknown Recrystallization-2 Handout Recrystallization-2 Movie  
5 Sept 21,22 Separatory Funnel and Rotory Evaporation:
Liquid/liquid Extraction; Extraction of Acids and Bases
Acid-Base Extraction Handout Acid-Base Extraction Movie  

Sept 28,29

Gas Chromatography-Mass Spectrometry (GC-MS) Lab GC-MS Handout GC-MS Movie  
7 Oct 5,6 Nucleophilic Substitution of Alkyl Halides
Mechanisms and Arrow Pushing
SN2-SN1 Handout SN2-SN1 Movie  
8 Oct 12,13 Chromatography;  TLC, Column, and Flash Chromatography Chromatography Handout Chromatography Movie  
9 Oct 19,20 Simple and Fractional Distillation of a Mixture Distillation Handout Distillation Movie  
10 Oct 26,27 C13 Nuclear Magnetic Resonance (C NMR) Spectroscopy C-13 NMR Handout
C-NMR Interpretation (Condensed)
C-13 Full Movie 80-min
11 Nov 2,3 1H Nuclear Magnetic Resonance (1H NMR) Spectroscopy
H-NMR Handout
H-NMR Interpretation (Condensed)
H-NMR Movie
  Nov 9,10 Makeup Lab. For any previously- cancelled lab days or labs that individuals missed Tuesday preferred, but Thursday allowed even though it's Veterans Day.  
12 Nov 16,17 Diels-Alder Reaction 1.Diels-Alder Reaction
2.Standard Synthesis Report Format
1.Diels-Alder Reaction Movie
2.Standard Synthesis Report Movie
  Nov 23,24 Thanksgiving No Lab even on Tuesday    
13 Nov 30, Dec 1 Nitration of Methyl Benzoate
Cleanup, Checkout
Nitration of Methyl Benzoate Handout Nitration of Methyl Benzoate Movie