Minnesota State University Moorhead
Dr. Craig P. Jasperse, Chemistry
Phone: (218) 477-2230            Home: (218) 291-9841 
Office: Hagen407J              email: jasperse@mnstate.edu           fax: (218) 477-2137
Office Hours:   Mon/Wed/Fri: 9-10:30, 1:00-2:00; Tues 10-11:30; Thurs 1:00-2:00

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Chem 342-Organic 2
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Full Chem 355 Lab Manual 2024
Chem 355 Syllabus for 2024

       Required Text and Materials for Fall 2024      

Chem 355 Lab Schedule Fall 2024   Full Chem 355 Lab Manual 2024
Ex Dates Experiment Expt. Links Movie Links  
1 Aug 29 Checkin, Melting Points Melting Range Handout Syllabus Movie
Melting Range Movie
-
2 Sept 5 Solubility Tests; Crystallization of Phtallic Acid
Recrystallizaton-1 Handout Recrystallizaton-1 Movie -
2 Sept 12 Molecular Structure Molecular Modelling Handout Molecular Modelling Movie -
4 Sept 19 Recrystallization of Acetanilide Using Mixed Solvent; Recrystallization of an Unknown Recrystallization-2 Handout Recrystallization-2 Movie  
5

Sept 26

Separatory Funnel and Rotory Evaporation:
Liquid/liquid Extraction; Extraction of Acids and Bases
Acid-Base Extraction Handout Acid-Base Extraction Movie  
6 Oct 3 Gas Chromatography-Mass Spectrometry (GC-MS) Lab GC-MS Handout GC-MS Movie  
7 Oct 10 Nucleophilic Substitution of Alkyl Halides
Mechanisms and Arrow Pushing
SN2-SN1 Handout SN2-SN1 Movie  
8 Oct 17 Chromatography;  TLC, Column, and Flash Chromatography Chromatography Handout Chromatography Movie  
9 Oct 24 Simple and Fractional Distillation of a Mixture Distillation Handout Distillation Movie  
10 Oct 31 C13 Nuclear Magnetic Resonance (C NMR) Spectroscopy C-13 NMR Handout
C-NMR Interpretation (Condensed)
C-13 Full Movie 76-min
 
11 Nov 7 1H Nuclear Magnetic Resonance (1H NMR) Spectroscopy
H-NMR Handout
H-NMR Interpretation (Condensed)
H-NMR Movie-Morning version 74-min
H-NMR Movie-Afternoon version 72-min
 
  Nov 14 Makeup Lab. For any previously- cancelled lab days or labs that individuals missed    
12 Nov 21 Diels-Alder Reaction 1.Diels-Alder Reaction
2.Standard Synthesis Report Format
1.Diels-Alder Reaction Movie
2.Standard Synthesis Report Movie, 2024 Version, 17 min,
Standard Synthesis Report Movie, earlier version: 10 min
 
  Nov 28 Thanksgiving No Lab even on Tuesday    
13 Dec 5 Nitration of Methyl Benzoate
Cleanup, Checkout
Nitration of Methyl Benzoate Handout Nitration of Methyl Benzoate Movie