Minnesota State University Moorhead
Dr. Craig P. Jasperse, Chemistry
Phone: (218) 477-2230            Home: (218) 291-9841 
Office: Hagen407J              email: jasperse@mnstate.edu           fax: (218) 477-2137
Office Hours:   Mon/Wed/Fri: 9-10:30, 1:00-2:00; Tues 10-11:30; Thurs 1:00-2:00

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Chem 355-O1 Lab
Chem 360-Organic 2
Chem 365-O2 Lab

Chem 341-Organic 1
Chem 342-Organic 2
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Syllabus Chem 365-2023                   Required Text and Materials        
2023 Complete Lab Manual (except for Research Module)
Standard Synthesis Lab Report Format
H-NMR Interpretation (Condensed)       H-NMR Interpretation (Longer)       NMR User's Manual
C13-NMR Interpretation (Condensed)        NMR Physics and C13-NMR (Longer)       GC/MS User's Manual

Chem 365 Lab Schedule Spring 2023
Lab times (Langseth 307): Thursday 9:00 pm  
THIS IS REVISED PLAN FOLLOWING FEB 23 STORM-CANCELLATION

Date Experiment Lab Manual for 2023 (Complete) (except research mod)
PreLab Lectures (Streaming)  
Jan 12 Cyalume: Chemiluminescence 1. Cyalume Experiment    
2. Syllabus

3. Standard lab report format
Syllabus and Introduction (6 min)
(2023 version)
Cyalume Prelab Lecture (26 min)
 
Jan 19 Grignard Reactions, Part 1 Grignard Reactions Grignard Prelab Week 1  
Jan 26 Grignard Reactions, Part II 1. Grignard Reactions
2. GC-MS User's Sheet
Grignard Prelab Week 2  
Feb 2 Alcohol to Ester; Catalysis; Distillation; NMR 1. Alcohol Esterification Expt
2. H-NMR Interpretation (Summary)
3. H-NMR Interpretation (Detailed)
4. NMR User's Sheet
Alcohol Esterification Prelab
How to Run the NMR
 
      NMR Movie: Format for reporting and interpreting H and C NMR  
    NMR Movie: How to find spectra for printing and processing  
Feb 9 Aspirin Synthesis/Alcohol Unknown (NMR) Aspirin, Alcohol NMR Expt 1. Aspirin, Alcohol Prelab
2. NMR: Standard Summary for H or C NMR
3. NMR: Finding spectra for printing and processing
 

Feb 16

Makeup Lab. For Making up previously-cancelled lab days or labs missed by individuals.    
Feb 23 SNOWED OUT
Sodium Borohydride Reduction of Ketone

SNOWED OUT
Sodium Borohydride Expt
Cyclohexane Chair Review and Video

Borohydride Reaction Prelab  
Mar 2 Sodium Borohydride Reduction of Ketone

Sodium Borohydride Expt
Cyclohexane Chair Review and Video

Borohydride Reaction Prelab  
Mar 9 Aldehydes and Ketones Unknown/Derivative Carbonyl Unknowns Experiment Carbonyl Unknowns Prelab  
Mar 16 Spring Break      
Mar 23 Dibenzalacetone by Aldol Condensation Aldol Reaction Experiment Aldol Prelab Video (24 min)  
Mar 30 Wittig Reaction Wittig Reaction Reaction Wittig Reaction Prelab (14 min)  
Apr 6 Snow Day      

Apr 13

Multistep Synthesis Research Module Week One
ORIGINALLY MAKEUP DAY

2023 READY
Research Module 2023 (full)

Week One Procedure
NMRs-for-video
ORIGINALLY MAKEUP DAY


Full Video, 54 min ...
-intro part
(15 min)
-part 1 procedure (16 min)
-Starting Scheme 2 procedure, including notes on Scheme 1 research report expectations (12 min)
-NMR part (10 min)

 
Apr 20 Multistep Synthesis Research Module Week Two

2023 READY
Research Module 2023 (full)

Week Two Procedure
NMRs-for-video

Week 2 video -44 min
1. Review and Overview, 1-14min
2. Procedure, 13-29 min
3. Lab Report, 29-33 min
4. NMR: 33-44 min

 
Apr 27 Amine Unknowns

Amines Unknown Experiment

Amines Prelab

 
Apr 27 Carboxylic Acid Unknown and Titration. Cleanup, Checkout Acid Unknowns Experiment

Acid Prelab Video (24 min)
 
         
      Full Video, 48 min ...
-intro part
(12min)
-procedure part (26min)
-NMR part (20 min)
-Starting Scheme 2 part
 
    Chem365-2020-Covid