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Chem 365 Lab Schedule Spring 2024
Lab times (Langseth 307): Thursday 9:00 pm AAA |
| Date |
Experiment |
Lab Manual for 2024 (Complete) (except research mod)
|
PreLab Lectures (Streaming) |
|
| Jan 11 |
Cyalume: Chemiluminescence |
1. Cyalume Experiment
2. Syllabus
3. Standard
lab report format |
Syllabus and Introduction (9 min)
(2024 version)
Cyalume Prelab Lecture (26 min) |
|
| Jan 18 |
Grignard Reactions, Part 1 |
Grignard Reactions |
Grignard Prelab Week 1 |
|
| Jan 25 |
Grignard Reactions, Part II |
1. Grignard Reactions
2. GC-MS User's Sheet |
Grignard Prelab Week 2 |
|
| Feb 1 |
Friedel Crafts Alkylation. |
Friedel Crafts Reaction |
Friedel Crafts Prelab |
|
| Feb 8 |
Alcohol to Ester; Catalysis; Distillation; NMR |
1. Alcohol Esterification Expt
2. H-NMR Interpretation (Summary)
3. H-NMR Interpretation (Detailed)
4. NMR User's Sheet |
Alcohol Esterification Prelab
How to Run the NMR |
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NMR Movie: Format for reporting and interpreting H and C NMR |
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NMR Movie: How to find spectra for printing and processing |
|
| Feb 15 |
Aspirin Synthesis/Alcohol Unknown (NMR) |
Aspirin, Alcohol NMR Expt |
1. Aspirin, Alcohol Prelab
2. NMR: Standard Summary for H or C NMR
3. NMR: Finding spectra for printing and processing |
|
| Feb 22 |
Sodium Borohydride Reduction of Ketone |
Sodium Borohydride Expt
Cyclohexane Chair Review and Video |
Borohydride Reaction Prelab |
|
| Feb 29 |
Aldehydes and Ketones Unknown/Derivative |
Carbonyl Unknowns Experiment |
Carbonyl Unknowns Prelab |
|
| Mar 7 |
Dibenzalacetone by Aldol Condensation |
Aldol Reaction Experiment |
Aldol Prelab Video (24 min) |
|
| Mar 14 |
Spring Break |
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| Mar 21 |
Wittig Reaction |
Wittig Reaction Reaction |
Wittig Reaction Prelab (23 min) |
|
| Mar 28 |
Makeup Lab. |
For Making up previously-cancelled lab days or labs missed by individuals. |
|
|
Apr 4 |
Multistep Synthesis Research Module Week One |
2024 READY
Research Module 2024 (full)
Week One Procedure
NMRs-for-video
|
Full Video, 52 min ...
-intro part (16 min)
-part 1 procedure (12 min)
-Starting Scheme 2 procedure, including notes on Scheme 1 research report expectations (13 min)
-NMR part (10 min)
|
|
| Apr 11 |
Multistep Synthesis Research Module Week Two
|
2024 READY
Research Module 2024 (full)
Week Two Procedure
NMRs-for-video
|
Week 2 procedure video -29 min
1. Review and Overview, 1-5min
2. Discussion of copper-catalyzed reaction mechanism, 5-9 min
3. Procedure, 9-29 min
Lab Report + NMR video - 25 min
4. Lab Report, 0-12 min
5. NMR:12-25 min
|
|
| Apr 18 |
Amine Unknowns
|
Amines Unknown Experiment
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Amines Prelab
|
|
| Apr 25 |
Carboxylic Acid Unknown and Titration. Cleanup, Checkout |
Acid Unknowns Experiment
|
Acid Prelab Video (24 min)
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Full Video, 48 min ...
-intro part (12min)
-procedure part (26min)
-NMR part (20 min)
-Starting Scheme 2 part |
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Chem365-2020-Covid |
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