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Chem 365 Lab Schedule Spring 2023
Lab times (Langseth 307): Thursday 9:00 pm
THIS IS REVISED PLAN FOLLOWING FEB 23 STORM-CANCELLATION
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| Date |
Experiment |
Lab Manual for 2023 (Complete) (except research mod)
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PreLab Lectures (Streaming) |
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| Jan 12 |
Cyalume: Chemiluminescence |
1. Cyalume Experiment
2. Syllabus
3. Standard
lab report format |
Syllabus and Introduction (6 min)
(2023 version)
Cyalume Prelab Lecture (26 min) |
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| Jan 19 |
Grignard Reactions, Part 1 |
Grignard Reactions |
Grignard Prelab Week 1 |
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| Jan 26 |
Grignard Reactions, Part II |
1. Grignard Reactions
2. GC-MS User's Sheet |
Grignard Prelab Week 2 |
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| Feb 2 |
Alcohol to Ester; Catalysis; Distillation; NMR |
1. Alcohol Esterification Expt
2. H-NMR Interpretation (Summary)
3. H-NMR Interpretation (Detailed)
4. NMR User's Sheet |
Alcohol Esterification Prelab
How to Run the NMR |
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NMR Movie: Format for reporting and interpreting H and C NMR |
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NMR Movie: How to find spectra for printing and processing |
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| Feb 9 |
Aspirin Synthesis/Alcohol Unknown (NMR) |
Aspirin, Alcohol NMR Expt |
1. Aspirin, Alcohol Prelab
2. NMR: Standard Summary for H or C NMR
3. NMR: Finding spectra for printing and processing |
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Feb 16 |
Makeup Lab. |
For Making up previously-cancelled lab days or labs missed by individuals. |
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| Feb 23 |
SNOWED OUT
Sodium Borohydride Reduction of Ketone |
SNOWED OUT
Sodium Borohydride Expt
Cyclohexane Chair Review and Video |
Borohydride Reaction Prelab |
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| Mar 2 |
Sodium Borohydride Reduction of Ketone |
Sodium Borohydride Expt
Cyclohexane Chair Review and Video |
Borohydride Reaction Prelab |
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| Mar 9 |
Aldehydes and Ketones Unknown/Derivative |
Carbonyl Unknowns Experiment |
Carbonyl Unknowns Prelab |
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| Mar 16 |
Spring Break |
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| Mar 23 |
Dibenzalacetone by Aldol Condensation |
Aldol Reaction Experiment |
Aldol Prelab Video (24 min) |
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| Mar 30 |
Wittig Reaction |
Wittig Reaction Reaction |
Wittig Reaction Prelab (14 min) |
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| Apr 6 |
Snow Day |
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Apr 13 |
Multistep Synthesis Research Module Week One
ORIGINALLY MAKEUP DAY
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2023 READY
Research Module 2023 (full)
Week One Procedure
NMRs-for-video
ORIGINALLY MAKEUP DAY
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Full Video, 54 min ...
-intro part (15 min)
-part 1 procedure (16 min)
-Starting Scheme 2 procedure, including notes on Scheme 1 research report expectations (12 min)
-NMR part (10 min)
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| Apr 20 |
Multistep Synthesis Research Module Week Two
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2023 READY
Research Module 2023 (full)
Week Two Procedure
NMRs-for-video
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Week 2 video -44 min
1. Review and Overview, 1-14min
2. Procedure, 13-29 min
3. Lab Report, 29-33 min
4. NMR: 33-44 min
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| Apr 27 |
Amine Unknowns
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Amines Unknown Experiment
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Amines Prelab
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| Apr 27 |
Carboxylic Acid Unknown and Titration. Cleanup, Checkout |
Acid Unknowns Experiment
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Acid Prelab Video (24 min)
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Full Video, 48 min ...
-intro part (12min)
-procedure part (26min)
-NMR part (20 min)
-Starting Scheme 2 part |
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Chem365-2020-Covid |
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