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Chem 365 Lab Schedule Spring 2020
Lab times (Langseth 307): Wedneday, 1:30pm, Thursday 9am, 1:30pm
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| Date |
Experiment |
Lab Manual for 2020 (Complete)
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PreLab Lectures (Streaming) |
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| Jan 13,14 |
Cyalume: Chemiluminescence |
1. Cyalume Experiment
2. Syllabus
3. Standard
lab report format |
Syllabus and Introduction (8 min)
Cyalume Prelab Lecture (27 min) |
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| Jan 20,21 |
Grignard Reactions, Part 1 |
Grignard Reactions |
Grignard Prelab Week 1 |
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| Jan 27,28 |
Grignard Reactions, Part II |
1. Grignard Reactions
2. GC-MS User's Sheet |
Grignard Prelab Week 2 |
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| Feb 3,4 |
Alcohol to Ester; Catalysis; Distillation; NMR |
1. Alcohol Esterification Expt
2. H-NMR Interpretation (Summary)
3. H-NMR Interpretation (Detailed)
4. NMR User's Sheet |
Alcohol Esterification Prelab |
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| Feb 10,11 |
No Lab/Makeup |
Unless Makeup Needed |
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NMR Movie: Format for reporting and interpreting H and C NMR |
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NMR Movie: How to find spectra for printing and processing |
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| Feb 17,18 |
Aspirin Synthesis/Alcohol Unknown (NMR) |
Aspirin, Alcohol NMR Expt |
1. Aspirin, Alcohol Prelab
2. NMR: Standard Summary for H or C NMR
3. NMR: Finding spectra for printing and processing |
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| Feb 224,25 |
Sodium Borohydride Reduction of Ketone |
Sodium Borohydride Expt
Cyclohexane Chair Review and Video |
Borohydride Reaction Prelab |
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| Mar 3,4 |
Aldehydes and Ketones Unknown/Derivative |
Carbonyl Unknowns Experiment |
Carbonyl Unknowns Prelab |
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| Mar 10,11 |
Spring Break |
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| Mar 17,18 |
COVID Break |
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| Mar 24,25 |
COVID Break |
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| Mar 31-Apr-1 |
Dibenzalacetone by Aldol Condensation |
Aldol Reaction Manual all ready |
Aldol Prelab Video (24 min)
Aldol Actual Experiment Video (30 min)
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|
| Apr 7,8 |
Wittig Reaction |
Wittig Reaction Manual all ready
Wittig Docx for Download |
Wittig Reaction Prelab (23 min)
Wittig Actual Experiment Video (40 min) |
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Apr 14,15 |
Multistep Synthesis Module Week One |
1. Report summary
2. Research Module 2020
3. Research Module docx
Ready to roll!
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Full Prelab Video, 58 min ... INcludes:
... -intro part (12min)
... -procedure part (26min)
... -NMR part (20 min)
Research Module 1 Experiment Video (37 min)
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|
| Apr 21,22 |
Multistep Synthesis Module Week Two
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1. Report summary
2. Research Module (PDF)
3. Research Module-2 docx
NMR and GC-MS Data for:
6aa, toluyl:
6ab, crotonyl:
6ac, benzoyl:
6ad, methoxy:
6ae, cinnamoyl:
Ready to roll!
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Week 2 video-28 min
Research Module 2 Experiment Video
(41 min)
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|
| Apr 28,29 |
Carboxylic Acid Unknown and Titration. Cleanup, Checkout |
1. Report summary
2. Acid Unknowns Experiment
3. Acid Unknowns Docx
NMR Data for:
Acid-A
Acid-B-C
Acid-D-G
Acid-H-K
Acid-L-N
Acid-O-S
Acid-T-Z
Ready to roll!
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Acid Prelab Video (24 min)
Acid Actual Experiment Video (26 min) |
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| Skip |
Research Module 3 |
Research Module 3 2020 |
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| Skip |
Amine Unknowns |
Amines Unknown Experiment |
Amines Prelab |
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