Minnesota State University Moorhead
Dr. Craig P. Jasperse, Chemistry
Phone: (218) 477-2230            Home: (218) 291-9841 
Office: Hagen 407J              email: jasperse@mnstate.edu           fax: (218) 477-2137
Office Hours:   Mon/Wed/Fri: 9-10:30, 1:00-2:00; Tues 10:30-12:00

Face-to-Face Courses
Chem 350-Organic 1
Chem 355-O1 Lab
Chem 360-Organic 2
Chem 365-O2Lab
Chem210-GenChem2
Chem 341-O1 NDSU
Chem 342-O2 NDSU

Online Organic Courses
AboutFall/SpringOnline
AboutSummerOnline
(Fall/Spring MSUM;
Summer NDSU)
Organic1-online-fall
Organic1-online-spring
Organic1-online-summer
Organic2-online-fall
Organic2-online-spring
Organic2-online-summer


email link to:
jasperse@mnstate.edu

Jasperse Home Page

NMR Tutorials+Movies

Prepharmacy

Personal

Research

 

 

 

 

 

 

 

NMR Usage Tutorials: Movies and Instruction Sheets
Note: if you'd like a movie and some saved/printable instructions customized for your research or class, let me know.
NMR Usage Guide: General 2-Page Instruction Guide for Software as of 2015

  Topic and Movie Pod Length
 Instruction Sheet Updated
1

NMR User's Guide: General Usage
-Pretty complete. Goes in order of User's Guide, so you can
fast forward to area of special interest
-Includes some explicit instrux for remote Concordia users

Pod 35min NMR User's Guide Oct 28, 2015
2 Sample Submission + Printing: Basic Pod 6 min UserGuide p1 Steps 7,8 Oct 28, 2015
3 Experiment Selection + Deletion Pod 4 min UserGuide p1 Step 6 Oct 28, 2015
4 Remote Control Submission/Printing (Concordia Interest) Pod 12 min UserGuide p1 Oct 28, 2015
5 Horizontal Expansions: Simple Zoom Pod 4 min UserGuide p2 #11 Oct 28, 2015
6 Horizontal Expansions: Research Precise/Advanced Pod 3 min UserGuide p1 #11,#14 Oct 28, 2015
7

Analytical: pKa Study (simple/short)
Analytical: pKa Study (detailed explanation)

Pod
Pod		 3 min
15 min		 pKa Study Steps (PDF)
Doc
 Nov 3, 2015
8 VT for PChem Lab Pod 7 min   2014
9 Updating Recent Completed Studies File Listing Pod 1 min PDF and Doc Nov 5, 2015
10

Operator Selection (Data Storage Folder Designation)

 Pod 2 min   Nov 5, 2015
11

Data File Retrieval
1) Right-clicking your node
2) From Completed Studies Folder
2) From the Data Folders

Pod 2 min   Nov 5, 2015
12 Solvent Suppression is Easy and Awesome!   5 min   2012
13 Running Multiple Experiments on a Single Sample   2 min   2012
14 Manual Integration and Integral Value Sets Pod 6 min UserGuide p2 #12,13 Nov 6, 2015
15 C-NMR Acquisition: Fundamental Steps   1 min   2012
16 Running Nuclei Other than C or H:
P, B, Sn, Pt, Si, Se, N, etc.. 		  3 min   2012
17

H-NMR Processing:
1) Horizontal Expansions (Zooming)
2) Manual Integration
3) Plotting to MSUM Printer
4) Sending Plots to Email Address

  4 min   2012
18 Prioritizing an Experiment in a Queue   1 min   2012
19 Editting a Sample that's already
been Submitted in a Queue		   1 min   2012

20

 Deleting a Sample from a Queue   1 min   2012
23 Cloning an Experiment or Study   4 min   2012
24 Stacking Plots via theViewport Tab (VJ4) pod 4 min   2013
25 Using Insets via the Frame Tab (VJ4) pod 3 min   2013
26 Customizing an Experiment.
When the Canned Settings aren't Optimal		   2 min   2012
27 H-NMR Acquisition: Fundamental Steps-(VJ4, 2013) Pod 5 min   2013
28

H-NMR Processing:
1) Horizontal Expansions (Zooming)
2) Manual Integration
3) Plotting to MSUM Printer
4) Sending Plots to Email Address

  4 min   2012
29

Basic Troubleshooting:

 Pod 6 min   2015
30

2D: Overview of Major 2D Experiments:
gCOSY (HH); ASAPHMQC (CC); zTOCSY (HH total)

  2 min   2012
31

2D Processing Fundamentals:
1) Adjusting scaling to get nice plots
2) Zooming (expanding to focus attention)
3) Viewing stacked plots (3D look)

pod 4 min   2012
32 2D: gCOSY. H-H Correlation
1) What it looks like
2) How to acquire		   4 min   2012
33 2D: ASAPHMQC. (HSQC, HMQC) C-H Correlation
1) What it looks like
2) How to acquire		   6 min   2012
34 2D: zTOCSY. H-H Correlation for Spin System
1) What it looks like
2) How to acquire
3) How it might be useful		   4 min   2012
35

Rapid Submission of Multiple Samples Doing the
Same Experiment:
1) All having same name (super fast)
2) With individualized sample names

  8 min   2012
36 VT Above 20º (Variable Temperature Basics)   5 min   2012
37 VT Below 20º (More Complex Variable Temperature)   4 min   2012
           
           
           
           
           
           
           
  Nitrogen NMR (unenriched) (Video deleted by mistake)        
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
           
          Podcasts Available
           
           
           
           
           
           
           
           
           
           
           
           
          Podcast: NMR Lecture 1